1H NMR spectroscopic study of the interaction between cyclodextrins and bicyclo[3.3.1]nonanes
✍ Scribed by Eugenius Butkus; José C. Martins; Ulf Berg
- Publisher
- Springer Netherlands
- Year
- 1996
- Tongue
- English
- Weight
- 546 KB
- Volume
- 26
- Category
- Article
- ISSN
- 0923-0750
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## Abstract Four derivatives of 2, 6, 6‐trimethylbicyclo[3.1.1]hept‐2‐ene (α‐pinene) and four derivatives of 2‐methylene‐6, 6‐dimethylbicyclo[3.1.1]heptane (β‐pinene) were synthesized and their ^1^H, ^13^C and ^17^O NMR spectra were measured, analysed and assigned. The ^1^H NMR spectral parameters
## Abstract Carbon‐13 NMR spectra of solid polycrystalline bicyclo[3.3.1]nonan‐9‐one and adamantanone have been measured at 315K. The relatively narrow ^13^C linewidths observed for these solids, together with measured spin‐lattice relaxation times, indicate that both these solids are orientational