1H NMR spectra of some 4,5-dihydro-1,2,4-triazol-5-ones
✍ Scribed by A. Aykut Ikizler; Aysun Ikizler; Haydar Yüksek
- Publisher
- John Wiley and Sons
- Year
- 1993
- Tongue
- English
- Weight
- 213 KB
- Volume
- 31
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
Abstract
Thirty 3‐substituted‐ and 3,4‐disubstituted‐4,5‐dihydro‐1,2,4‐triazol‐5‐ones (seven being new compounds) were synthesized and their proton magnetic resonance spectra were measured in trifluoroacetic acid (TFA). The protonation shifts observed on comparison of the spectra run in DMSO‐d~6~ and TFA were attributed to an amidinium‐type resonance of the resulting cations in the acidic medium.
📜 SIMILAR VOLUMES
1997 triazole derivatives triazole derivatives R 0280 ## 09 -110 A Study on 4,5-Dihydro-1H-1,2,4-triazol-5-ones. -Phthalimides like (V) are obtained by the reaction of the title triazoles (IV) with phthalic anhydride at high temperature. In the case of compound (I) and (VI) the reaction gives the