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1H NMR resonance assignments in a paramagnetic heme protein by two-dimensional spectroscopy: Heme resonances in equine met-azido myoglobin

✍ Scribed by David H. Peyton


Book ID
115764421
Publisher
Elsevier Science
Year
1991
Tongue
English
Weight
343 KB
Volume
175
Category
Article
ISSN
0006-291X

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Assignment of resonances in the 1H spect
✍ Kevin L. Behar; Takashi Ogino πŸ“‚ Article πŸ“… 1991 πŸ› John Wiley and Sons 🌐 English βš– 1011 KB

Two-dimensional shift-correlated (COSY) and J-resolved NMR spectroscopy was used to identify and assign resonance in the aliphatic region (0.8 to 4.5 ppm) of the 1H spectrum of acid extracts and tissue of rat brain. The chemical shift and spin-spin coupling constants of several resonances, which cou