Assignment of the 31P and 1H resonances in oligonucleotides by two-dimensional NMR spectroscopy
✍ Scribed by Vladimir Sklenár̆; Hirotsugu Miyashiro; Gerald Zon; H. Todd Miles; Ad Bax
- Book ID
- 115918847
- Publisher
- Elsevier Science
- Year
- 1986
- Tongue
- English
- Weight
- 350 KB
- Volume
- 208
- Category
- Article
- ISSN
- 0014-5793
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Two-dimensional shift-correlated (COSY) and J-resolved NMR spectroscopy was used to identify and assign resonance in the aliphatic region (0.8 to 4.5 ppm) of the 1H spectrum of acid extracts and tissue of rat brain. The chemical shift and spin-spin coupling constants of several resonances, which cou
## Abstract The identity and structures of warifteine and methylwarifteine, two tertiary bisbenzylisoquinoline alkaloids of an unusual type, were elucidated and verified by 2D NMR spectroscopy. Complete ^1^H and ^13^C NMR spectral assignments were obtained. Copyright © 2003 John Wiley & Sons, Ltd.