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1H and13C NMR analysis of some trichothecenes

✍ Scribed by Markku Mesilaakso; Maija Moilanen; Erkki Rahkamaa

Publisher
Springer
Year
1989
Tongue
English
Weight
732 KB
Volume
18
Category
Article
ISSN
0090-4341

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A general strategy, using well established techniques, is outlined for the assignment of signals in the 13C NMR spectra of the trichothecene mycotoxins and some related rearrangement products. Heteronuclear NOE difference spectra were employed to assign resonances from quaternary carbons. An example

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