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13C NMR spectra of some trichothecene mycotoxins and derivatives

✍ Scribed by Anthony G. Avent; John Frederick Grove; James R. Hanson

Publisher
John Wiley and Sons
Year
1988
Tongue
English
Weight
538 KB
Volume
26
Category
Article
ISSN
0749-1581

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✦ Synopsis

A general strategy, using well established techniques, is outlined for the assignment of signals in the 13C NMR spectra of the trichothecene mycotoxins and some related rearrangement products. Heteronuclear NOE difference spectra were employed to assign resonances from quaternary carbons. An example of the use of spin-echo J modulation is given.

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