## Abstract ^1^H and ^13^C NMR spectra were studied for a number of 1,8‐bis(dimethylamino)naphthalene (DMAN) salts in acetonitrile‐__d__~3~. In the case of strong acids no counter anion effect was observed on the protonated DMAN molecules. A splitting of the ^1^H signal of the CH~3~ groups was foun
1H and 13C Solid-State NMR Studies of 1,8-Bis(dimethylamino)naphthalene and Its Complexes
✍ Scribed by Wozniak, Krzysztof; He, Heyong; Klinowski, Jacek; Grech, Eugeniusz
- Book ID
- 120584700
- Publisher
- American Chemical Society
- Year
- 1995
- Tongue
- English
- Weight
- 637 KB
- Volume
- 99
- Category
- Article
- ISSN
- 0022-3654
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## Abstract Hydrogen and carbon‐13 NMR chemical shifts of five complexes of 1,8‐bis(dimethylamino)naphthalene with strong acids were measured in acetonitrile‐__d__~3~ and nitromethane‐__d__~3~ and identified by 2D, NOE difference and long‐range enhanced COSY spectra. The assignments of the resonanc
An ionic complex of 1,8-bis(dimethylamino)naphthalene with picrolonic acid was studied by C and 1 H magic angle spinning and x-ray diffraction. Structural and spectroscopic features of this compound were investigated. The detailed x-ray structure of this complex is described. A multicentre model of