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1H and 13C NMR spectroscopy of 6-aryl-substituted 3-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-s-triazolo[3,4-b]-1,3,4-thiadiazoles

✍ Scribed by Heng-Shan Dong; Bin Quan; Kun Wei; Qing-Lian Wang; Zi-Yi Zhang

Publisher: John Wiley and Sons
Year: 2000
Tongue: English
Weight: 93 KB
Volume: 38
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(200003)38:3<210::aid-mrc616>3.0.co;2-s

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✦ Synopsis

Novel 6-aryl-3-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-s-triazolo[3,4-b]-1,3,4-thiadiazoles were synthesized by the condensation of 3-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-4amino-5-mercapto-s-triazole with various aromatic carboxylic acids in the presence of phosphorus oxychloride. The compounds were characterized by MS, IR, 1 H and 13 C NMR spectroscopy. The measured and calculated 13 C chemical shifts of the aromatic carbons were compared.

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