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1H and 13C NMR spectral data of bioactive cage-like polycyclic compounds

✍ Scribed by Roberta C. Salles; Valdemar Lacerda Jr; Adilson Beatriz; Felicia M. Ito; Reginaldo B. dos Santos; Sandro J. Greco,; Eustáquio V. R. de Castro; Dênis P. de Lima

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
176 KB
Volume
48
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

Bioactive cage‐like polycyclic compounds have attracted the attention of several research groups because of their unique appearance and their biological activities. Their structures were established on the basis of ^1^H NMR and ^13^C NMR spectroscopic data. The ^1^H and ^13^C signal assignments and most homonuclear hydrogen coupling constants were assigned by use of techniques such as 1D ^1^H and ^13^C NMR and 2D gCOSY, non‐edited gHSQC and gHMBC. The gNOESY experiments proved the endo‐stereochemistry. Copyright © 2010 John Wiley & Sons, Ltd.

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