0 'H-and 'W-NMR data and spectral assignments are reported for fenobam using noise modulated gated, single frequency off resonance, and single frequency selective proton decoupling techniques. Keyphrases 0 Fenobam-'H-and 13C-NMR spectroscopic analysis 0 'H-and 'T-NMR spectroscopy-analysis of fenoba
1H and 13C NMR spectra of pseudomorphine and dimethylpseudomorphine
✍ Scribed by D. W. Graden; G. W. Caldwell; F. J. Villani; C. A. Maryanoff; A. Grant
- Publisher
- John Wiley and Sons
- Year
- 1990
- Tongue
- English
- Weight
- 355 KB
- Volume
- 28
- Category
- Article
- ISSN
- 0749-1581
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
The ^1^H and ^13^C NMR spectra of 7,7′,8,8′‐tetradehydro‐4,5:4′,5′‐diepoxy‐17,17′‐dimethyl‐[2,2′‐bimorphinan]‐3,3′,6,6′‐tetrol; [2,2′‐bimorphine] (pseudomorphine) and 7,7′,8,8′‐tetradehydro‐4,5:4′,5′‐diepoxy‐17,17′‐dimethyl‐[2,2′‐bimorphinan]‐3,3′‐dimethoxy‐6,6′‐diol; 2,2′‐bimorphine (dimethylpseudomorphine) were measured and assigned using DEPT, COSY, HETCOR, NOESY, NOE difference techniques and selective proton decoupled carbon NMR experiments.
📜 SIMILAR VOLUMES
Proton and carbon-13 spectra of benzyl compounds of the general formula (C,H,CH,),X with a large variety of X substituents have been measured. While a linear relationship between the CH, chemical shift and the substituent electronegativity was found both for lH and lac, large deviations from lineari
The 'H NMR and 13C NMR spectra of neopentyl and benzyl substituted disulfides, thiosulfinates, thiosulfonates, thiols, sulfides, sulfinic acids and sulfonic acids are reported. The deshielding electron withdrawing effects of -SO, -SO,, -SOz-, -SO,H, -SO,-, S 0 , H and S03CH3 on or-ðylene and benz
A set of 3-alkylaminoacroleins (R1NHCHxCHCHxO, R1 \ alkyl) were studied by 13C and 1H NMR spectroscopy in solutions of di †erent solvents and, for the simplest representative of the series, 3methylaminoacrolein, at di †erent temperatures. The equilibrium solutions of these compounds consists of mixt
(1)H and (13)C NMR data for N-substituted morpholines 1-20 were measured using 1D (DEPT, 1D NOE difference) and 2D NMR spectroscopic methods including (1)H-(1)H COSY, long-range (1)H-(1)H COSY, NOESY, gHMBC and gHMQC experiments. At room temperature the (1)H NMR spectra of protonated compounds 2 and