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1H and 13C NMR spectra of N-substituted morpholines

✍ Scribed by Alan R. Katritzky; Novruz G. Akhmedov; Hongfang Yang; C. Dennis Hall


Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
89 KB
Volume
43
Category
Article
ISSN
0749-1581

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✦ Synopsis


(1)H and (13)C NMR data for N-substituted morpholines 1-20 were measured using 1D (DEPT, 1D NOE difference) and 2D NMR spectroscopic methods including (1)H-(1)H COSY, long-range (1)H-(1)H COSY, NOESY, gHMBC and gHMQC experiments. At room temperature the (1)H NMR spectra of protonated compounds 2 and 9 show the chair conformation for the morpholine ring. Spin-spin coupling constants were deduced from the resolution-enhanced proton spectra.


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