The complete proton assignments of the aminoglycoside antibiotics, butirosin A, kanamycin A and kanamycin B, at pH 6.5 have been made through the use of various homonuclear and heteronuclear 2D NMR methods. Butirosin A NOESY experiments suggest a stacking arrangement between the xylose and 2,6-diami
✦ LIBER ✦
1D- and 2D-NMR spectroscopy studies of the polysaccharide gum from Spondias purpurea var. lutea
✍ Scribed by Omaira Gutiérrez de G; Maritza Martı́nez; Lilian Sanabria; Gladys León de Pinto; J.Manuel Igartuburu
- Book ID
- 113627074
- Publisher
- Elsevier Science
- Year
- 2005
- Tongue
- English
- Weight
- 211 KB
- Volume
- 19
- Category
- Article
- ISSN
- 0268-005X
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## Abstract A procedure for the estimation of the mixing time between the last two 90° pulses in the classic three‐pulse sequence NOESY/EXSY is proposed and tested and some considerations for the treatment of the two‐dimensional (2D) ^1^H NMR exchange spectra are given. The rate constants are thus