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1—Azatriene cyclisation as a route to annelated pyrido[4,3-b]indoles

✍ Scribed by Thomas L. Gilchrist; Paul D. Kemmitt; Andrew L. Germain


Publisher
Elsevier Science
Year
1997
Tongue
French
Weight
671 KB
Volume
53
Category
Article
ISSN
0040-4020

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A new synthetic route to the azocino[4,3
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## Abstract The reaction of 2 with 2‐methoxyethylamine in the presence of ZnCl~2~ afforded imine 3, which was reduced with NaBH~4~ to amine 4 without isolation. After deprotection of the carbonyl function by treatment with benzeneseleninic anhydride, ketone 5 was converted to compound 6 with 2‐oxob