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1,8-Bis(3-formyl-5-methyl-2-oxido­benzyl)-1,8-diaza-4,11-diazo­niacyclo­tetra­decane chloro­form solvate

✍ Scribed by Gayathri, D. ;Velmurugan, D. ;Ravikumar, K. ;Sreedaran, S. ;Narayanan, V.

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
189 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 28 H 40 N 4 O 4 ÁCHCl 3 , crystallizes with two half-molecules of the macrocycle and one molecule of chloroform solvent in the asymmetric unit. Each macrocycle lies on a centre of inversion. The molecular structure is stabilized by N-HÁ Á ÁO and C-HÁ Á ÁO intramolecular interactions, and the crystal packing is stabilized by C-HÁ Á ÁO and C-HÁ Á Á intermolecular interactions.

📜 SIMILAR VOLUMES

2-(4-Chloro-3-methyl­phen­oxy)-3-(4-chlo
2-(4-Chloro-3-methyl­phen­oxy)-3-(4-chloro­phen­yl)-5-methyl-8,9,10,11-tetra­hydro-1-benzothieno[2′,3′:2,3]pyrido[4,3-d]pyrimidin-4(3H)-one dichloromethane solvate
✍ Liu, Jian-Chao ;He, Hong-Wu ;Ding, Ming-Wu 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 180 KB

2-(4-Chloro-3-methylphenoxy)-3-(4-chlorophenyl)-5-methyl-8,9,10,11-tetrahydro-1-benzothieno-[2 0 0 0 ,3 0 0 0 :2,3]pyrido [4,3-d]pyrimidin-4(3H)-one dichloromethane solvate

13-Benzyl-3,10-bis(2,6-di­chloro­phenyl)
13-Benzyl-3,10-bis(2,6-di­chloro­phenyl)-4,11-di­phenyl-1,8-dioxa-2,9,13-tri­aza­di­spiro­[4.1.4.3]­tetradeca-2,9-dien-6-one chloro­form solvate
✍ Li, Xiao-Fang ;Feng, Ya-Qing ;Hu, Xiao-Fen ;Xu, Mian 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 183 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.009 A Ê Disorder in solvent or counterion R factor = 0.064 wR factor = 0.196 Data-to-parameter ratio = 14.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.