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13-Benzyl-4,11-bis-(4-chloro­phenyl)-3,10-bis(2,6-di­chloro­phenyl)-1,8-dioxa-2,9,13-tri­aza­di­spiro­[4.1.4.3]­tetradeca-2,9-dien-6-one chloro­form solvate

✍ Scribed by Li, Xiao-Fang ;Feng, Ya-Qing ;Gao, Bo ;Li, Nan

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
185 KB
Volume
59
Category
Article
ISSN
1600-5368

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13-Benzyl-3,10-bis(2,6-di­chloro­phenyl)
13-Benzyl-3,10-bis(2,6-di­chloro­phenyl)-4,11-di­phenyl-1,8-dioxa-2,9,13-tri­aza­di­spiro­[4.1.4.3]­tetradeca-2,9-dien-6-one chloro­form solvate
✍ Li, Xiao-Fang ;Feng, Ya-Qing ;Hu, Xiao-Fen ;Xu, Mian 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 183 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.009 A Ê Disorder in solvent or counterion R factor = 0.064 wR factor = 0.196 Data-to-parameter ratio = 14.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

4,11-Bis(4-chloro­phenyl)-3,10-bis(2,6-d
4,11-Bis(4-chloro­phenyl)-3,10-bis(2,6-di­chloro­phenyl)-1,8-dioxa-2,9-di­aza­di­spiro­[4.1.4.4]­pentadeca-2,9-dien-6-one
✍ Li, Xiao-Fang ;Feng, Ya-Qing ;Xiao-Fen, Hu ;Mian, Xu 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 159 KB

The title compound, C 35 H 24 Cl 6 N 2 O 3 , which was synthesized by the [3 + 2]-cycloaddition of 2,6-dichlorobenzonitrile oxide and 2,7-bis(4-chlorobenzylidene)cycloheptanone, contains two independent molecules in the asymmetric unit. Three rings are linked by two spiro-C atoms. The cycloheptanone

4,11-Bis(4-methoxy­phenyl)-3,10-bis(2,6-
4,11-Bis(4-methoxy­phenyl)-3,10-bis(2,6-di­chloro­phenyl)-1,8-dioxa-2,9-di­aza­di­spiro­[4.1.4.3]­tetra­deca-2,9-dien-6-one–chloro­form–methanol (2/2/1)
✍ Li, Xiao-Fang ;Feng, Ya-Qing ;Gao, Bo ;Li, Nan 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 151 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.007 A Ê Disorder in solvent or counterion R factor = 0.068 wR factor = 0.232 Data-to-parameter ratio = 14.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.