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17β-Hydroxy-4,14-androstadien-3-one

✍ Scribed by Rohrer, D. C. ;Strong, P. D. ;Duax, W. L. ;Segaloff, A.


Book ID
114525444
Publisher
International Union of Crystallography
Year
1978
Weight
293 KB
Volume
34
Category
Article
ISSN
0567-7408

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17β-Hydroxy-4,14-estradien-3-one
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Preparation of 17β-hydroxy-[1ξ,2ξ-3H2]4,
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## Abstract 17β‐Hydroxy‐[1ξ,2ξ‐^3^H~2~]4,6‐androstadien‐3‐one was prepared by the selective reduction of 17β‐hydroxy‐1,4,6‐androstatrien‐3‐one in benzene with tritium over 5% palladium on carbon. After purification by thin layer chromatography and high pressure liquid chromatography, the specific a