Measurement of 15N–1H bond lengths by ro
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Riqiang Fu
📂
Article
📅
2003
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Elsevier Science
🌐
English
⚖ 220 KB
A method based on rotational-echo double-resonance (REDOR) NMR is proposed to measure 1 H-15 N bond lengths under magic-angle-spinning. Protons are selectively polarized and evolve under the frequency-switched Lee-Goldburg (FSLG) homonuclear decoupling, while two 15 N p pulses are applied to restore