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15N NMR spectra, tautomerism and diastereomerism of 4,5-dihydro-1H-1,2,3-triazoles

Book ID
121313254
Publisher
Royal Society of Chemistry
Year
2001
Tongue
English
Weight
458 KB
Volume
1
Category
Article
ISSN
1472-779X

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## Abstract Thirty 3‐substituted‐ and 3,4‐disubstituted‐4,5‐dihydro‐1,2,4‐triazol‐5‐ones (seven being new compounds) were synthesized and their proton magnetic resonance spectra were measured in trifluoroacetic acid (TFA). The protonation shifts observed on comparison of the spectra run in DMSO‐__d

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N NMR chemical shifts were measured for a series of substituted 5-amino-1,2,4-triazoles. The assignment of isomeric structures agrees with earlier results obtained with the use of proton-coupled I3C NMR.