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140. Tetrahedral nickel(II) complexes and the factors determining their formation. Part I. Bistriphenylphosphine nickel(II) compounds

✍ Scribed by Venanzi, L. M.

Book ID: 115475796
Publisher: The Royal Society of Chemistry
Year: 1958
Weight: 558 KB
Category: Article
ISSN: 0368-1769
DOI: 10.1039/jr9580000719

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Formation and Dissociation of Tetrahedra

Formation and Dissociation of Tetrahedral Nickel(II) and Cobalt(II) Complexes of ‘Dithioimidodiphosphato’ Ligands, Measurement of Kinetically Determined Stability Constants, and Kinetic Investigations of the Rapid Formation of Tetrahedral Bis(ligand)copper(II) Complexes and Their Rates of Reduction to Trinuclear Copper(I) Species

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## Abstract The stopped‐flow technique was used to measure the rates of formation and dissociation of tetrahedral [ML~2~] complexes (M^2+^=Ni^2+^ or Co^2+^) of four bidentate S~2~‐donor ‘dithioimidodiphosphato’ ligands L^−^ (HL=[R^1^R^2^P(S)]NH[P(S)R^3^R^4^], R^1^ to R^4^=alkyl) at 25.0° in MeOH/