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1,4-Diphenylbutadiyne as a potential tritium getter

✍ Scribed by H.H. Miller; E.R. Bissell; R.T. Tsugawa; P.C. Souers

Publisher: Elsevier Science
Year: 1980
Weight: 76 KB
Volume: 31
Category: Article
ISSN: 0020-708X
DOI: 10.1016/0020-708x(80)90271-9

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## Abstract Five steps were required to synthesize the title compound. This involved a catalytic exchange reaction, nitration, hydrolysis, and condensation. The overall radiochemical yield was 28.87% and the specific activity was 12.4 mCi/mmol, with a radiochemical purity of more than 95.7%.