The recoupling of ~3C-IH dipolar interactions by applying ~3C pulses under a ~H decoupling rf field is discussed. It is theoretically and experimentally shown that ]3C spectral line-broadening due to such recoupling in a ]3C "n-pulse train can be minimized by setting the rf field intensity for ~H de
13C13C Dipolar interactions provide a mechanism for obtaining resonance assignments in solid state 13C NMR spectroscopy
✍ Scribed by Philip E Pfeffer; Kevin B Hicks; Michael H Frey; Stanley J Opella; William L Earl
- Publisher
- Elsevier Science
- Year
- 1983
- Weight
- 202 KB
- Volume
- 55
- Category
- Article
- ISSN
- 0022-2364
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