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13C-NMR studies of marine natural products II. Total assignment of the 13C-NMR spectrum of asperdiol

✍ Scribed by Gary E. Martin; James A. Matson; Alfred J. Weinheimer

Publisher: Elsevier Science
Year: 1979
Tongue: French
Weight: 206 KB
Volume: 20
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)93674-3

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✦ Synopsis

13 C-nmr spectral assignments for asperdiol are made with the aid of model compounds and Tl relaxation behavior.

Overall isotropic tumbling was inferred from the latter providing a supplemental means of multiplicity determination.

Utilization of the Tl relaxation times as an assignment criterion

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