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13C n.m.r. relaxation study of poly(aspartic acid)

✍ Scribed by H. Pivcová; V. Saudek


Publisher
Elsevier Science
Year
1985
Tongue
English
Weight
482 KB
Volume
26
Category
Article
ISSN
0032-3861

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Synthesis of DL-[2-13C, 15N]aspartic aci
✍ Robert L. Baxter; Elaine M. Abbot 📂 Article 📅 1985 🏛 John Wiley and Sons 🌐 French ⚖ 205 KB

A synthesis of the title compound from /13Clparaformaldehyde and [15N)ammonium chloride V f 8 ethyl 2-(1 ,3-/2-13Cldithianyl) acetate 3a is described. Ethyl/3-13C13-oxopropanoate derived in sl'tu from 3a was converted by a stepwise Strecker procedure to DL-[ 2-13C,15Nlaspartic acid 7a.