13C-Edited Double-Quantum Spectroscopy of Peptides and Proteins
β Scribed by J. Balbach; H. Kessler
- Publisher
- Elsevier Science
- Year
- 1994
- Tongue
- English
- Weight
- 340 KB
- Volume
- 105
- Category
- Article
- ISSN
- 1064-1866
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## Abstract Several new protonβdetected heteronuclear twoβdimensional (2D) nmr techniques are presented that exhibit the features of __selection__ and __editing__ of multiplicity. The theoretical basis of the new features is briefly discussed and the application of the 2D techniques to a thioanalog
Four small type I collagen CNBr peptides containing complete natural sequences were purified from bovine skin and investigated by CD and 1H- and 13C-nmr spectroscopies to obtain information concerning their conformation and thermal stability. CD showed that a triple helix was formed at 10 degrees C