13C Chemical shifts which obey the Curie Law in CP/MAS NMR spectra. The first CP/MAS NMR chemical-shift thermometer
β Scribed by Gordon C Campbell; Richard C Crosby; James F Haw
- Publisher
- Elsevier Science
- Year
- 1986
- Weight
- 301 KB
- Volume
- 69
- Category
- Article
- ISSN
- 0022-2364
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π SIMILAR VOLUMES
The spinning sidebands observed in the 13 C MAS NMR spectra (Fig. 1a), oriented in a nematic phase and in the solid state of cis,cis-mucononitrile oriented in liquid-crystalline media and of are presented. As a consequence of the carbon-13 chemicalthe neat sample in the solid state are studied. Ther
We demonstrate a dipolar-chemical shift correlation technique for sign-sensitive determination of the torsion angle in solid peptides and proteins under magic-angle spinning. The indirect dimension of the experiment is obtained by separate but synchronous evolution of the magnetization under the 15