Determination of the Peptide Torsion Ang
✍
M. Hong; J.D. Gross; W. Hu; R.G. Griffin
📂
Article
📅
1998
🏛
Elsevier Science
🌐
English
⚖ 214 KB
We demonstrate a dipolar-chemical shift correlation technique for sign-sensitive determination of the torsion angle in solid peptides and proteins under magic-angle spinning. The indirect dimension of the experiment is obtained by separate but synchronous evolution of the magnetization under the 15