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1,3-Shifts. IV. The Kinetics of the Thermal Rearrangement of α-Phenethyl Chlorocarbonates 1

✍ Scribed by Wiberg, Kenneth B.; Shryne, Thomas M.

Book ID: 121370683
Publisher: American Chemical Society
Year: 1955
Tongue: English
Weight: 602 KB
Volume: 77
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01615a031

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B 371 1 -Ethynyl-2,2,3,3-tetramethylcyclopropane (9) has been prepared and subjected to gas phase pyrolysis. Above 200°C the hydrocarbon rearranges to 4,4,5-trimethyl-I ,2,5-hexatriene (10) and 5,6dimethyl-5-hepten-I-yne (11). Whereas the allene is produced directly from 9 by a 1,Shydrogen shift, th