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1,3-Diphosphacyclobutadienecobalt(I) Complexes from Phosphaalkynes

✍ Scribed by Priv.-Doz. Dr. Paul Binger; Dipl.-Chem. Roman Milczarek; Dr. Richard Mynott; Prof. Dr. Manfred Regitz; Dipl.-Chem. Wolfgang Rösch

Book ID
101554010
Publisher
John Wiley and Sons
Year
1986
Tongue
English
Weight
249 KB
Volume
25
Category
Article
ISSN
0044-8249

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Preparation of 1,3-diphosphabuta-1,3-die
Preparation of 1,3-diphosphabuta-1,3-dienes from sterically encumbered phosphaalkyne and phosphaethenyllithium
✍ Shigekazu Ito; Hideaki Miyake; Hiroki Sugiyama; Masaaki Yoshifuji 📂 Article 📅 2005 🏛 John Wiley and Sons 🌐 English ⚖ 107 KB

## Abstract Kinetically stabilized 2‐lithio‐1‐(2,4,6‐tri‐t‐butylphenyl)‐1‐phosphapropene was allowed to react with a bulky phosphaalkyne Mes\*CP (Mes\* = 2,4,6‐t‐Bu~3~C~6~H~2~) followed by quenching with iodomethane or benzyl bromide to give the corresponding 1,3‐diphosphabuta‐1,3‐dienes. The pres