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1,3-Bis(tri-tert-butylsilyl)triazene

✍ Scribed by Prof. Dr. Nils Wiberg; Dr. Gerd Fischer; Petros Karampatses


Publisher
John Wiley and Sons
Year
1984
Tongue
English
Weight
226 KB
Volume
23
Category
Article
ISSN
0044-8249

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pounds, presumably oligomers. In glacial acetic acid (CH3C0,H/CH2C12=3 :2, i=40 mA/cm2, T=2OoC, Pt electrode) 17% androstanyl acetate is obtained and 38% androstane is recovered. Remarkable is the selectivity of the oxidation: We found that the 6-(6a), 7-, and 12-acetates are formed in the ratio 35

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