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1,3-Bis(phenylmercapto)propane and 1-chloro-3-(phenylmercapto)propane: useful precursors for 1,3-dilithiopropane synthons in the preparation of 1,5-diols

✍ Scribed by Francisco Foubelo; Miguel Yus *


Book ID
108379824
Publisher
Elsevier Science
Year
2000
Tongue
French
Weight
203 KB
Volume
41
Category
Article
ISSN
0040-4039

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## Abstract magnified image A solid support under microwave (MW) irradiation without solvent allowed the synthesis of the 2,3‐epoxy‐propyl‐thioimidazole **4**, regioselectively, and prohibited its cyclization to give the imidazo[2,1‐__b__]thiazine **3** from the reaction of 4,5‐diphenylimidazole‐2