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1,2-Isopropylidene Glycerol Carbonate: Preparation, Characterization, and Hydrolysis

✍ Scribed by James A. Kenar; Gerhard Knothe

Book ID
107491277
Publisher
Springer-Verlag
Year
2008
Tongue
English
Weight
272 KB
Volume
85
Category
Article
ISSN
0003-021X

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πŸ“œ SIMILAR VOLUMES

An improved method for the preparation o
An improved method for the preparation of 1,2-isopropylidene-SN-glycerol
✍ HansjΓΆrg Eibl πŸ“‚ Article πŸ“… 1981 πŸ› Elsevier Science 🌐 English βš– 258 KB

A simple and fast route for the preparation of 1,2-isopropylidene-sn-glycerol from Dmannitol in 45% yield is described. The value of optical rotation, [a] ~ + 15.2 Β°, is higher than usual indicating considerable racemization for other procedures, Since 1,2-isopropylidene-sn-glycerol serves as genera

Resolution of isopropylidene-glycerol be
Resolution of isopropylidene-glycerol benzoate by sequential enzymatic hydrolysis and preferential crystallization
✍ Daniele Bianchi; Aldo Bosetti; Paolo Golini; Pietro Cesti; Carlo Pina πŸ“‚ Article πŸ“… 1997 πŸ› Elsevier Science 🌐 English βš– 194 KB

Both enantiomers of isopropylidene-glycerol are prepared from its benzoate ester with enantiomeric excess \_>95% by combined partially stereoselective lipasecatalyzed hydrolysis and preferential crystallization. (~) 1997 Elsevier Science Ltd. All rights reserved.