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1,1,2,2,9,9,10,10-Octamethyl-1,2,9,10- tetragerma[2.2]paracyclophane: the first [2.2]paracyclophane bridged by two GeGe bonds

✍ Scribed by Akira Sekiguchi; Tetsuo Yatabe; Chizuko Kabuto; Hideki Sakurai

Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
317 KB
Volume
390
Category
Article
ISSN
0022-328X

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Full multinuclear resonance analysis of
Full multinuclear resonance analysis of 4-amino-1,1,2,2,9,9,10,10-octafluoro[2.2]paracyclophane
✍ Alex J. Roche; Alexander A. Marchione; Sheryl A. Rabinowitz 📂 Article 📅 2005 🏛 John Wiley and Sons 🌐 English ⚖ 183 KB

The complete assignment of 19 F, 1 H and 13 C NMR spectra for a monosubstituted octafluoro[2.2]paracyclophane derivative is described for the first time. The unambiguous assignments were achieved through the combination of 19 F-1 H HOESY, 1 H COSY and 19 F COSY techniques and then further confirmed

The ESR. Spectrum of the Radical Anion o
The ESR. Spectrum of the Radical Anion of 1,1,2,2,9,9,10,10-Octafluoro [2.2]paracyclophane
✍ Fabian Gerson; Hiroaki Ohya-Nishiguchi; Georges Plattner 📂 Article 📅 1982 🏛 John Wiley and Sons 🌐 German ⚖ 278 KB

## Abstract The radical anion of 1,1,2.2,9,9,10, 10‐octafluoro[2.2]paracyclophane (**1**) has been generated by electrolytic reduction of **1** in 1,2‐dimethoxyethane (tetrabutylammonium perchlorate as the supporting salt). The hyperfine coupling constants of the eight ^19^F‐nuclei and the eight pr