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1,10-Phenanthrolinium perchlorate

✍ Scribed by Shang, Run-Ling ;Du, Lin ;Sun, Bai-Wang

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
143 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The proton-transfer title compound, C~12~H~9~N~2~
^+^·ClO~4~
^−^, has been obtained from 1,10-phenanthroline and HClO~4~. In the crystal structure, the molecules stack along the a axis via hydrogen-bond interactions and van der Waals forces.

📜 SIMILAR VOLUMES

1,10-Phenanthroline pyridinium perchlora
1,10-Phenanthroline pyridinium perchlorate
✍ Tai, Xi-Shi ;Yin, Jie ;Feng, Yi-Min 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 237 KB

Single-crystal X-ray study T = 294 K Mean (C-C) = 0.005 A R factor = 0.053 wR factor = 0.139 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Primary cycloadducts of 1,10-phenanthrol
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✍ Florea Dumitraşcu; Carmen Irena Mitan; Constantin Drăghici; Miron Teodor Căproiu 📂 Article 📅 2001 🏛 Elsevier Science 🌐 French ⚖ 155 KB

Primary cycloadducts cis-2 and trans-6 of monosubstituted cycloimmonium phenacylides 1 and 5 with DMAD have been obtained for the first time. They isomerise stereospecifically and regiospecifically by prototropic rearrangement to dihydro derivatives cis-3 and trans-7, respectively. The new heterocyc