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1,1′-Bis(methylphenylphosphanyl)ferrocene: Synthesis and Complexes with the Tetracarbonylchromium Fragment

✍ Scribed by Herberich, Gerhard E. ;Moss, Stefan

Publisher: Wiley (John Wiley & Sons)
Year: 1995
Tongue: English
Weight: 518 KB
Volume: 128
Category: Article
ISSN: 0009-2940
DOI: 10.1002/cber.19951280706

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✦ Synopsis

1,l'-Bis(methylphenylphosphany1)ferrocene (mppf) (2) was 2)Cr(C0)4 (meso-5) were obtained photochemically from hesynthesized from dilithioferrocene and PMePh(OC6H4-4-xacarbonylchromium and mppf in near quantitative yield. Me). The diastereomers rac-2 and meso-2 were separated by The structures of rac-2, rac-5, and meso-5 were determined fractional crystallization from ethanol. The tetracarbonyl-by X-ray crystallographic analysis. chromium complexes (ra~-2)Cr(CO)~ (rac-5) and (meso-

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