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103. Synthesis of norharmancarboxylic acid and its bearing on the constitution of lysergic acid

โœ Scribed by King, Harold ;Stiller, Eric T.


Book ID
120274411
Publisher
The Royal Society of Chemistry
Year
1937
Weight
984 KB
Category
Article
ISSN
0368-1769

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The preparation of lysergic acid -die.thylmnide i s described. 14C -Diethylamine was synthesised i n three steps; ## sodium / 4 C l # ~c e t a t e was treated with thionyl chloride giving [14CI)-acetyZ chZoride which WIS reacted with ethylmnine t o give -N-ethyl-(14Cl]-acetwiide. Reduction of t h i