1-aza-spiro annelation, II: A synthetic approach to 1-aza-spiro[4.4]nonanes.
✍ Scribed by T.A. Bryson; D.C. Smith; S.A. Krueger
- Book ID
- 104243799
- Publisher
- Elsevier Science
- Year
- 1977
- Tongue
- French
- Weight
- 191 KB
- Volume
- 18
- Category
- Article
- ISSN
- 0040-4039
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
The title compound, C 6 H 8 N 2 O 3 S 2 ÁH 2 O, was synthesized from l-erythrulose and the structure of the enantiopure (4R,9S) diastereoisomer has been determined. The structure is a hydrate and the water molecules establish a hydrogen-bond network that involves the hydroxymethyl group as well as o
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.005 A Ê R factor = 0.085 wR factor = 0.287 Data-to-parameter ratio = 15.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 200 K Mean '(C±C) = 0.011 A Ê R factor = 0.054 wR factor = 0.142 Data-to-parameter ratio = 8.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.009 A Ê R factor = 0.068 wR factor = 0.198 Data-to-parameter ratio = 9.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.