3-Benzyl-7,7-dimethyl-9-phenyl-1-thia-3-aza-7-azoniaspiro[4.4]nonane-2,4-dione iodide
✍ Scribed by Li, Xiao-Fang ;Feng, Ya-Qing ;You, Xu-Dong ;Xu, Mian
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 133 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.009 A Ê R factor = 0.068 wR factor = 0.198 Data-to-parameter ratio = 9.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 6 H 8 N 2 O 3 S 2 ÁH 2 O, was synthesized from l-erythrulose and the structure of the enantiopure (4R,9S) diastereoisomer has been determined. The structure is a hydrate and the water molecules establish a hydrogen-bond network that involves the hydroxymethyl group as well as o
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.005 A Ê R factor = 0.085 wR factor = 0.287 Data-to-parameter ratio = 15.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.054 wR factor = 0.131 Data-to-parameter ratio = 15.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.006 A Ê R factor = 0.079 wR factor = 0.195 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.