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[μ-trans-N,N′-Bis(3-amino­prop­yl)oxamidato(2–)]bis­[(methanol)picratocopper(II)]

✍ Scribed by Song, Yu-Lan ;Li, Yan-Tuan ;Wu, Zhi-Yong ;Zhang, Gui-Ling ;Sun, Fen

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
299 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

trans-N,N 0 0 0 -Bis(3-aminopropyl)oxamidato(2-)]bis[(methanol)picratocopper(II)]

📜 SIMILAR VOLUMES

Bis{μ-1-[bis­(3-amino­prop­yl)amino]prop
Bis{μ-1-[bis­(3-amino­prop­yl)amino]propan-2-olato}zinc(II) bis(perchlorate)
✍ Zhang, Zhenming ;Gao, Jian ;Wang, Daqi ;Xu, Tongtao 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 108 KB

Single-crystal X-ray study T = 298 K Mean (C-C) = 0.011 A Disorder in solvent or counterion R factor = 0.054 wR factor = 0.098 Data-to-parameter ratio = 12.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

trans-Bis[(2E)-3-(N,N-dimethyl­amino)-1-
trans-Bis[(2E)-3-(N,N-dimethyl­amino)-1-(2-pyrid­yl)prop-2-en-1-one-κ2N,O]bis­(perchlorato-κO)cadmium(II)
✍ Hu, Tong-Liang ;Tian, Jin-Lei 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 171 KB

In the title compound, [Cd(ClO 4 ) 2 (C 10 H 12 N 2 O) 2 ], the Cd atom (site symmetry 1) is trans-coordinated by two N,O-bidentate chelating (2E)-3-(N,N-dimethylamino)-1-(2-pyridyl)prop-2en-1-one ligands, and by two O atoms from two perchlorate anions, in a slightly distorted octahedral geometry.