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μ-3,3′-Bisacetyl­acetonato-bis­[(1,10-phenanthroline)palladium(II)] bis(hexa­fluoro­phosphate) acetonitrile solvate

✍ Scribed by Mei, Guang-Quan ;Huang, Ke-Long ;Huang, Hai-Ping

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
221 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

l-3,3 0 0 0 -Bisacetylacetonato-bis[(1,10-phenanthroline)palladium(II)] bis(hexafluorophosphate) acetonitrile solvate

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Single-crystal X-ray study T = 223 K Mean '(C±C) = 0.005 A Ê R factor = 0.045 wR factor = 0.105 Data-to-parameter ratio = 27.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.012 A Ê R factor = 0.089 wR factor = 0.172 Data-to-parameter ratio = 8.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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✍ Herres-Pawlis, Sonja ;Flörke, Ulrich ;Henkel, Gerald 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 299 KB

Di-l-fluoro-bis[(acetonitrile){N,N 0 0 0 -bis[(dimethylamino)(morpholino)methylene]propane-1,3-diamine}copper(II)] bis(hexafluorophosphate): the first di-l-fluoro-bridged dicopper bisguanidine compound

Di-μ-iodo-bis­[(1,10-phenanthroline-κ2N,
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In the title complex, [Cu 2 I 2 (C 12 H 8 N 2 ) 2 ]ÁC 2 H 3 N, two Cu I atoms are bridged by two I atoms and each Cu I atom is chelated by a 1,10-phenanthroline ligand to give four-coordinate tetrahedral geometry.