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α-tributylstannylacetals: Preparation via transacetalisation of diethoxymethyltributyltin, and use for the synthesis of new α-stannylated ethers

✍ Scribed by Alain Duchêne; Sophie Boissière; Jean-Luc Parrain; Jean-Paul Quintard

Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
747 KB
Volume
387
Category
Article
ISSN
0022-328X

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✍ Shatzmiller, Shimon ;Dolithzky, Ben-Zion ;Bahar, Eliezer 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 English ⚖ 502 KB

## Abstract The synthesis of optically pure chloromethyl (−)‐menthyl ether (2b) and its use in the synthesis of di‐(−)‐menthyl acetal (−)‐menthyl (+)‐menthyl acetals are described. The diastereomeric mixed acetals 7a, b and 8a, b are easily obtainable from the nitrones 5 and 6, KCN and 2b. The mixt