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α-Arylation of Aldehydes Via α-Chloroaldimines

✍ Scribed by Norbert De Kimpe; Yao Zi-Peng¶; Niceas Schamp

Book ID
102773562
Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
772 KB
Volume
98
Category
Article
ISSN
0037-9646

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The construction of a cycloalkyl ring at the e-position of rldehydes by cycktion of o-Moaldimincs is descrii. Akylatioa of the corrcspondirg aldiiincs with a,o-diihaloallanes follawcd by treatment with LDA results in a convenient acccas to o,a-cyclobkakykted akliiincs which are hydrolyzed to the a+-