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(α-Aminoalkyl)cuprates Prepared from Soluble Copper(I) Salts: Conjugate Additions to α,β-Unsaturated Carboxylic Acid Derivatives

✍ Scribed by Dieter, R. Karl; Velu, Sadanandan E.

Book ID: 120663832
Publisher: American Chemical Society
Year: 1997
Tongue: English
Weight: 155 KB
Volume: 62
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo970443u

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and treated with lBuCl (1.18 g, 12.8 mmol) directly after filtration. The mixture was stirred at room temperature for 12 h before the orange solution was evaporated to dryness. Recrystallization of the residue from toluene (ca. 30 mL) affords a yellow crystalline powder (2.50 g, 40%). which decompos