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Zur Umsetzung vonN-substituiertenN′-Chloramidinen mit Kalium-S-methyl-N-cyanimidodithiocarbonat — eine neue Thiadiazolsynthese

✍ Scribed by Sonnenschein, Helmut ;Walek, Wolfgang ;Schmitz, Ernst ;Reck, Günter


Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
229 KB
Volume
1992
Category
Article
ISSN
0947-3440

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✦ Synopsis


Reaction of N‐Substituted N′‐Chlorobenzamidines with Potassium S‐Methyl N‐Cyanimidodithiocarbonate — a New Thiadiazole Synthesis

In contrast to a known procedure for the synthesis of 1,2,4‐thiadiazoles 3 from N‐unsubstituted N′‐chlorobenzamidines 1a and potassium S‐methyl cyanimidodithiocarbonate (2) the substituted amidines 1b–1e form thiadiazoles 5a–d containing both nitrogen atoms of amidines in the ring system.