Zur Aminoalkylierung des β-Tetralons
✍ Scribed by Prof. Dr. H. J. Roth; F. Assadi
- Book ID
- 101631824
- Publisher
- John Wiley and Sons
- Year
- 1970
- Tongue
- English
- Weight
- 300 KB
- Volume
- 303
- Category
- Article
- ISSN
- 0365-6233
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
Recently we described a simple method for the preparation of g-tetmlone-3carboxylates' using magnesium methyl carbomte.2r3 In connection with this work we 2230 cm.-' (CN), 1760 cm.-' (enol acetate), 1680 cm.-' (C=(Z); x max 202 mp (29,ooO), 275 mp (21@), 281 mp (2400); r 6. I7 (3H\_singlet, -08&), '
## One of the best methods for synthesizing 6-tetralones is that reported by 8urkhalter.l The reaction consists of mixing a phenylacetyl chloride and AlCl, in carbon disulfide, then bubbling in ethylene for several hours at 0'. However, in our hands, the product obtained in