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Zirconium-Catalyzed Oxidation of Primary Aliphatic Amines to Nitro Compounds with tert-Butyl Hydroperoxide

✍ Scribed by Karsten Krohn; Jochen Küpke

Publisher: John Wiley and Sons
Year: 1998
Tongue: English
Weight: 360 KB
Volume: 1998
Category: Article
ISSN: 1434-193X
DOI: 10.1002/(sici)1099-0690(199804)1998:4<679::aid-ejoc679>3.0.co;2-w

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✦ Synopsis

Primary aliphatic amines are oxidized with tert-butyl hydroperoxide to the corresponding nitro compounds in 50Ϫ98% yield using Zr(Ot-Bu) 4 as the catalyst. The CH-acidic nitro

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