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Zinc?acetic acid reduction of the steroid 4-en-3-one: novel conversion of the 4-en-3-one into the 2-en-4-one via a vinyl chloride

✍ Scribed by Templeton, John F.; Majid, Samar; Marr, Angelina; Marat, Kirk

Book ID
121422318
Publisher
Royal Society of Chemistry
Year
1990
Weight
440 KB
Volume
9
Category
Article
ISSN
1472-7781

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📜 SIMILAR VOLUMES

The 0.893/0.104/0.003 cocrystal of 1-(4-
The 0.893/0.104/0.003 cocrystal of 1-(4-methyl­phen­yl)-3-(3,4,5-trimethoxy­phen­yl)prop-2-en-1-one, 3-(3-chloro-4,5-dimethoxy­phen­yl)-1-(4-methyl­phen­yl)prop-2-en-1-one and 3-(3,5-dichloro-4-methoxy­phen­yl)-1-(4-methyl­phen­yl)prop-2-en-1-one
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In the title cocrystal, 0.893C 19 H 20 O 4 Á0.104C 18 H 17 ClO 3 Á-0.003C 17 H 14 Cl 2 O, the crystal packing is stabilized by weak intermolecular C-HÁ Á ÁO and C-HÁ Á Á interactions.

The azo–en­amino­ne 4-(E)-amino-3-[(E)-2
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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.060 wR factor = 0.185 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.