Zero-Valent Palladium Complexes with Mon
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Alexander M. Kluwer; Cornelis J. Elsevier; Michael Bühl; Martin Lutz; Anthony L.
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Article
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2003
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John Wiley and Sons
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English
⚖ 124 KB
General procedure: To a mixture of dry THF (10 mL) and the appropriate N ligand (5 mL) was added solid [(h 2 ,h 2 -nbd)(h 2 -ma)Pd 0 ] (0.15 g, 0.5 mmol). In the case of ammonia, 3-4 mL was condensed at À70 8C, to which cold THF (10 mL) was slowly added, followed by the Pd 0 complex as above. After