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Ytterbium Coordination Polymer with Four Different Coordination Numbers: The First Structural Characterization of Lanthanide Phthalate Complex

✍ Scribed by Yong-Hong Wan; Lin-Pei Jin; Ke-Zhi Wang

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
318 KB
Volume
20
Category
Article
ISSN
0256-7660

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✦ Synopsis

Abstract

The novel ytterbium coordination polymer is a two‐dimensional framework in which the central metal ions have four different coordination numbers and form four kinds of coordination polyhedra. The four kinds of coordination polyhedra connect into infinite chains by sharing oxygen atoms.

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New lead(II)-saccharin complexes, [Pb(sac) 2 (pym)] (1) and [Pb(sac) 2 (pydm)] (2) (sac Ο­ saccharinate anion; pym Ο­ 2-pyridylmethanol; pydm Ο­ pyridine-2,6-dimethanol) were synthesized and characterized by IR spectroscopy and single crystal X-ray diffractometry. Complex 1 crystallizes in the monoclin