X-ray structures of iron(III) and cobalt(III) complexes containing 2-S-methyl-6-methyl-4-formylpyrimidine-N(4)-ethylthiosemicarbazone
✍ Scribed by Sachindranath Pal; Anil Kumar Barik; Prahlad Aich; Shie-Ming Peng; Gene-Hsiang Lee; Susanta Kumar Kar
- Publisher
- Springer
- Year
- 2006
- Tongue
- English
- Weight
- 308 KB
- Volume
- 18
- Category
- Article
- ISSN
- 1040-0400
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As part of a programme involving X-ray crystallographic studies" of cis-and tpuns-fused hexopyranosides, we now report on the crystal structures of methyl 2-~-methyl-~-D-glucop~anoside\* (11, which was obtained by debe~lidenation of methyl 4,~-O-benzyIidene-2-O-methyI-3-O-~-tolylsulfonyl-~-~-glucopy
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.011 A Ê R factor = 0.061 wR factor = 0.139 Data-to-parameter ratio = 19.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.