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X-ray structure analysis and molecular conformation of tert-butyloxycarbonyl-L-prolylproline (Boc-Pro-Pro): errata

โœ Scribed by Kamwaya, M. E. ;Oster, O. ;Bradaczek, H.

Book ID
114528159
Publisher
International Union of Crystallography
Year
1982
Weight
88 KB
Volume
38
Category
Article
ISSN
0567-7408

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Crystal structure and molecular conformation of N-boc-L-pro-dehydro-leu-OCH3
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The peptide N-Boc-L-Pro-dehydro-Leu-OCH3 was synthesized by coupling dehydroleucine methyl ester with Boc-Pro-OH. It was crystallized from its solution in a methanol-water mixture at 4ยฐC and the crystals belong to the orthorhfmbic space group P2,2,2, with a = 10.239( 1) A, b = 19.276(4) A, c = 20.31

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The peptide N-Boc-L-Pro-dehydro-Phe-L-Gly-OH was synthesized by the usual workup procedure and finally coupling the N-Boc-L-Pro-dehydro-Phe to glycine. The geptide crystallizes monoclinic space group P2: with a = 8.951( ) A, b = 5.677(6) A, c = 21.192(11) A, p = 96.97(4)', V = 1069(1) A3, Z = 2, d,